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    Innovative procedure for precise deposition of wrinkled hydrogel films using direct inkjet printing

    Year: 2020

    Journal: Mater. Des., Volume 194, SEP

    Authors: Gonzalez-Henriquez, Carmen M.; Rodriguez-Umanzor, Fernando E.; Sarabia-Vallejos, Mauricio A.; Terraza, C. A.; Martinez-Campos, Enrique; Rodriguez-Hernandez, Juan

    Organizations: FONDECYTComision Nacional de Investigacion Cientifica y Tecnologica (CONICYT)CONICYT FONDECYT [1170209]; FONDEQUIP [EQM150101]; CONICYTComision Nacional de Investigacion Cientifica y Tecnologica (CONICYT); Ministerio de Ciencia, Innovacion y Universidades [RTI2018-096328-B-I00]; Ministerio de Ciencia, Innovacion y Universidades (FONDOS FEDER) [MAT2016-78437-R]

    Keywords: Inkjet printing; Drop-on-demand deposition; Wrinkled hydrogel films; Hierarchical patterns

    This manuscript presents an inkjet-based strategy to fabricate wrinkled hydrogel surfaces with controlled characteristics (period and amplitude). For this purpose, a monomer mixture containing a crosslinking agent, a hydrophilic monomer, and a photoinitiator were deposited onto polycarbonate substrates. Upon UV irradiation and controlled drying under a vacuum atmosphere, either one-generation or hierarchical two-generation wrinkles were formed. More interestingly, the wrinkle characteristics depend on the crosslinking agent and monomer concentration in the solution so that larger wrinkles were observed in diluted solutions. Equally, the wrinkle period and amplitude also gradually grow by increasing the number of deposited layers. Atomic force microscopy was carried out to finely characterize the wrinkle dimensions as well as their eventual preferential orientation and distribution. Besides, hydrogel surfaces have been evaluated in terms of cytocompatibility, given their potential interest for biomedical applications. (c) 2020 The Authors. Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
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