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In Situ Synthesis of Palladium Nanoparticles in Polymer Brushes Followed by QCM-D Coupled with Spectroscopic Ellipsometry

Year: 2013

Journal: Particle & Particle Systems Characterization Special Issue: Remotely Controlled Colloids, Interfaces, and Biosystems Volume 30, Issue 11, pages 931–935, November 2013, 20140105

Authors: Meike Koenig 1 2, Keith Brian Rodenhausen 3, Daniel Schmidt 4, Klaus-Jochen Eichhorn 1, Mathias Schubert 4, Manfred Stamm 1 2, Petra Uhlmann 1 *

Last authors: Petra Uhlmann

Organizations: 1 Leibniz Institute of Polymer Research Dresden, Dresden, Germany 2 Department of Physical Chemistry of Polymer Materials, Technische Universität Dresden, Dresden, Germany 3 Department of Chemical and Biomolecular Engineering, University of Nebraska-Lincoln, NE, USA 4 Department of Electrical Engineering, University of Nebraska-Lincoln Lincoln, NE, USA

Country: USA, US, United States, United States of America, America, Germany

The combinatorial method of quartz crystal microbalance coupled with spectroscopic ellipsometry can be used to follow the in situ synthesis of catalytically active palladium nanoparticles in polymer brushes in situ. By combining these two orthogonal techniques, it is possible to thoroughly characterize the thickness, composition, optical, and mechanical properties of nanoscopic thin films.