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    Properties of gelatin-based films incorporated with chitosan-coated microparticles charged with rutin

    Year: 2017

    Journal: Int. J. Biol. Macromol., Volume 101, AUG, page 643–652

    Authors: Dammak, Ilyes; Quinta Barbosa Bittante, Ana Monica; Lourenco, Rodrigo Vinicius; do Amaral Sobral, Paulo Jose

    Organizations: Sao Paulo Research Foundation (FAPESP) [CEPID FoRC 13/07914-8, 15/02879-5]; Brazilian National Council for Scientific and Technological Development (CNPq) [30.0799/2013-6]

    Keywords: Encapsulation; Chitosan; Microparticles

    The aim of this study was development an active film based on gelatin incorporated with antioxidant, rutin carried into microparticles. The complexation between oppositely charged lecithin and chitosan was applied to prepare the chitosan-coated microparticles. The generated microparticles had an average size of 520 +/- 4nm and a span of 0.3 were formulated by a rotor-stator homogenize at the homogenization speed 10,000 rpm. Composite films were prepared by incorporating chitosan-coated microparticles, at various concentrations (0.05, 0.1, 0.5, or 1% (based on the weight of the gelatin powder)) in the gelatin based films. For the prepared films, the results showed that obtained physicochemical, water vapor barrier, and mechanical were compared with native gelatin film with a slight decrease for chitosan concentration higher than 0.5%. The microstructure studies done by scanning electron microscopes, revealed different micropores embedded with oil resulting from the incorporation of the microparticles into the gelatin matrix. Moreover, the calorimetric results were comparable to those of gelatin control film with Tg value 45 degrees C and increased crystallinity percentage with increasing incorporation of microparticles. This original concept of composite biodegradable films may thus be a good alternative to incorporate liposoluble active compounds to design an active packaging with good properties. (C) 2017 Elsevier B.V. All rights reserved.
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